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• W2113222806 startingPage "1785" @default.
• W2113222806 abstract "Abstract Tris- and bis-ligand complexes of nickel(II) with S-benzyldithiocarbazate (SBDTC) having the general formulae Ni(SBDTC) 3 X 2 ·H 2 O (X = Cl, Br and NO 3 ) and Ni(SBDTC) 2 X 2 (X = Cl and NCS), respectively, were synthesized and characterized by electronic and IR spectroscopy and magnetic measurements. The ligand acts as a bidentate sulphur-nitrogen chelating agent. Both the tris- and bis-ligand cationic nickel(II) complexes are high-spin with magnetic moments of ca. 3.10 B.M. On the basis of magnetic and spectral evidence octahedral structures are assigned to these complexes. Under alkaline conditions complexes of the deprotonated ligand having the formulae M(SBDTCA) 2 [M = Ni(II) and Zn(II); SBDTCA = anion of SBDTC] were isolated. The nickel(II) complex is square-planar. The Schiff base CH=N-NHCSS 2 C 6 H 5 (NNSH)forms intensely coloured crystalline complexes with nickel(II) and copper(II) having the general formula M(NNS)X [M = Ni(II) and Cu(II); X = Cl, Br or NO 3 and NNS is the anion of NNSH]. The nickel(II) complexes are diamagnetic. The magnetic behaviour of the Cu(NNS)X (X = Cl and Br) complexes over the temperature range 320-93°K obeys the Curie-Weiss law. The variable-temperature magnetic data coupled with IR and electronic spectral evidence support square-planar stereochemistries for the copper(II) complexes." @default.
• W2113222806 created "2016-06-24" @default.
• W2113222806 creator A5054258574 @default.
• W2113222806 creator A5087590930 @default.
• W2113222806 date "1977-01-01" @default.
• W2113222806 modified "2023-10-18" @default.
• W2113222806 title "Metal complexes of sulphur and nitrogen-containing ligands: Complexes of s-benzyldithiocarbazate and a schiff base formed by its condensation with pyridine-2-carboxaldehyde" @default.
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• W2113222806 doi "https://doi.org/10.1016/0022-1902(77)80202-9" @default.
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