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- W2113276870 abstract "The relationship of the injector and column and its influence on GC conditions, method detection limits, resolution, and analysis times for total petroleum hydrocarbon analyses are examined. Decreasing the length and diameter of the capillary column results in a significant analysis time reduction. The resolution of closely eluting peaks is maintained or improved with smaller columns. Even with very short analysis times, the chromatographic profiles or patterns of different petroleum samples are still easily distinguishable. For Megabore direct injectors, the best solvent front shapes and widths are obtained with flash vaporization liners, allowing the resolution of very light hydrocarbons from the solvent front. Packing the liner with glass wool improves the peak shape of the heavier, low-volatility hydrocarbons. The use of split injectors results in increases in method detection limits and injector discrimination. As column diameter decreases, the use of faster ramp rates in the temperature program is required to obtain the shortest analysis times." @default.
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- W2113276870 date "1999-11-01" @default.
- W2113276870 modified "2023-09-25" @default.
- W2113276870 title "Total Petroleum Hydrocarbon Analysis by Capillary Gas Chromatography: Decreasing Analysis Times Using Small-Diameter Columns" @default.
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- W2113276870 doi "https://doi.org/10.1093/chromsci/37.11.448" @default.
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