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• W2113306216 startingPage "1690" @default.
• W2113306216 abstract "Abstract In this study, a silicic acid and tetra isopropyl ortho titanate ceramic precursor and a metallocene polyethylene‐octene elastomer (POE) or acrylic acid grafted metallocene polyethylene‐octene elastomer (POE‐g‐AA) were used in the preparation of hybrids (POE/SiO 2 TiO 2 and POE‐g‐AA/SiO 2 TiO 2 ) using an in situ sol‐gel process, with a view to identifying a hybrid with improved thermal and mechanical properties. Hybrids were characterized using Fourier transform infrared spectroscopy, 29 Si solid‐state nuclear magnetic resonance (NMR), X‐ray diffraction, differential scanning calorimetry, thermogravimetry analysis, dynamic mechanical thermal analysis, and Instron mechanical testing. Properties of the POE‐g‐AA/SiO 2 TiO 2 hybrid were superior to those of the POE/SiO 2 TiO 2 hybrid. This was because the carboxylic acid groups of acrylic acid acted as coordination sites for the silica‐titania phase to allow the formation of stronger chemical bonds. 29 Si solid‐state NMR showed that Si atoms coordinated around SiO 4 units were predominantly Q 3 and Q 4 . The 10 wt % SiO 2 TiO 2 hybrids gave the maximum values of tensile strength and glass transition temperature in both POE/SiO 2 TiO 2 and POE‐g‐AA/SiO 2 TiO 2 . It is proposed that above this wt %, excess SiO 2 TiO 2 particles caused separation between the organic and inorganic phases. © 2005 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 43: 1690–1701, 2005" @default.
• W2113306216 created "2016-06-24" @default.
• W2113306216 creator A5090701944 @default.
• W2113306216 date "2005-03-04" @default.
• W2113306216 modified "2023-10-18" @default.
• W2113306216 title "Synthesis of polyethylene-octene elastomer/SiO2-TiO2 nanocomposites via in situ polymerization: Properties and characterization of the hybrid" @default.
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• W2113306216 doi "https://doi.org/10.1002/pola.20649" @default.
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