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• W2113419013 abstract "The reactions of CoX2 (X 5 Br, Cl) with the planar, bidentate bridging ligand 2,1,3-benzothiadiazole (btd) in Me2CO led to the 2D coordination polymers M[CoBr2(btd)]Nn (1) and M[CoCl2(btd)]Nn (2). The structure of 1 was determined by singlecrystal X-ray crystallography. Complex 1 (C6H4Br2CoN2S, monoclinic, P21/m, a 5 3.742(3), b 5 13.075(9), c 5 9.092(6) As , b 5 90.09(2)3, Z 5 2, h+2h, R1 5 0.0298, wR2 5 0.0793) consists of M[Co(l-Br)2]Nn linear chains running along the a axis linked via l-btd ligands along the b axis. The columns of stacked btd molecules present in the crystal structure of the free ligand are maintained in the lattice of 1. XRD data revealed that 2 is isostructural with 1. The magnetic properties of both complexes can be explained by the presence of a very weak ferromagnetic intrachain Co2Co exchange interaction through the (l-X)2 bridges and a moderate antiferromagnetic Co2Co interaction through the l-btd bridges. The new complexes were also characterized by EPR, IR, and UV/VIS spectra, and all data are discussed in terms of the nature of bonding and known structures. ( 2001 Academic Press" @default.
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• W2113419013 date "2001-07-01" @default.
• W2113419013 modified "2023-09-26" @default.
• W2113419013 title "Topological Control in Two-Dimensional Cobalt(II) Coordination Polymers by π–π Stacking Interactions: Synthesis, Spectroscopic Characterization, Crystal Structure, and Magnetic Properties" @default.
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• W2113419013 doi "https://doi.org/10.1006/jssc.2001.9167" @default.
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