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- W2113646700 abstract "A process for double deuterium labeling of an alcohol was developed. The process was utilized in the subsequent tritium labeling of a secondary alcohol with high specific activity (24 Ci/mmol) by reduction of the corresponding ketone using sodium borotritide. The starting ketone was first brominated with pyridinium tribromide; the resulting alpha bromoketone was then reduced in THF/alcohol in the presence of Ni(OAc)2. The alcohol was then converted to 2-amino-4-fluorobicyclo[3.1.0]hexane-2,6-dicarboxylic acid-[3H2], an mGluR agonist. Copyright © 2004 John Wiley & Sons, Ltd." @default.
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- W2113646700 date "2004-08-01" @default.
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- W2113646700 title "A method for the synthesis of 2-amino-4-fluoro-bicyclo[3.1.0]hexane-2,6-dicarboxylic acid-[3H2]" @default.
- W2113646700 doi "https://doi.org/10.1002/jlcr.843" @default.
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