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- W2113759568 abstract "A 31P and 13C NMR study of powder and single crystal samples of two phosphoenolpyruvate (PEP) compounds, the tris-ammonium salt monohydrate (NH4)3(PEP)·H2O (1), and the mono-ammonium-salt (NH4)(H2PEP) (2) is presented. The P chemical shielding tensors in 1 are measured by 31P single crystal NMR on four minuscule samples and assigned without ambiguity by exploiting the orientation-dependent 31P-31p dipolar splittings of the resonance lines. The orientation of the 31P chemical shielding tensor is discussed in terms of the C2v — and C3-type distortions of the phosphate PO4-coordination sphere. From 13C MAS NMR experiments with 31P rotary resonance recoupling on polycrystalline powder samples the orientations of the 31P chemical shielding tensors in 1 and 2 are obtained, for 1 in very good agreement with the 31P single crystal NMR results. Only some of the orientational parameters of the three 13C chemical shielding tensors in the PEP moiety of 1 could be derived from 13C MAS NMR experiments with 31P rotary resonance recoupling." @default.
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- W2113759568 date "2000-05-10" @default.
- W2113759568 modified "2023-09-26" @default.
- W2113759568 title "31P and13C chemical shielding tensors in the phosphoenolpyruvate moiety from rotary resonance recoupling13C and31P MAS and single crystal31P NMR" @default.
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- W2113759568 doi "https://doi.org/10.1080/00268970009483327" @default.
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