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- W2114842172 abstract "Abstract Two ternary borates, Na3CaB5O10 and Na3MgB5O10, have been prepared by solid-state reactions at temperature below 750 °C. Single-crystal X-ray structural analyses showed that Na3CaB5O10 crystallizes in the triclinic space group P 1 ¯ with a = 7.4403(6) A, b = 9.7530(10) A, c = 12.9289(9) A, α = 90.972(7)°, β = 90.073(7)°, γ = 109.656(6)°, Z = 4 and Na3MgB5O10 in the orthorhombic group Pbca with a = 7.838(1) A, b = 12.288(1) A, c = 18.180(2) A, Z = 8. Na3CaB5O10 has a superstructure, with the cell volume being two times of that reported previously. The crystal structure consists of discrete [B5O10]5− anions separated by six-coordinated Ca2+ as well as five-, six- and seven-coordinated Na+ cations. Na3MgB5O10 contains [B5O10]5− groups that are bridged by MgO4 tetrahedra through common O atoms to form 2D [ MgB 5 O 10 ] 3 − ∞ 2 layers, with Na+ cations situated between and within the layers. The IR spectra further confirmed the presence of BO3 and BO4 groups in both compounds." @default.
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- W2114842172 date "2007-11-20" @default.
- W2114842172 modified "2023-09-25" @default.
- W2114842172 title "Syntheses and Crystal Structures of Two Pentaborates, Na3CaB5O10 and Na3MgB5O10." @default.
- W2114842172 cites W2950684312 @default.
- W2114842172 doi "https://doi.org/10.1002/chin.200747005" @default.
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