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• W2114958512 abstract "A measurement system capable of continuous on-line matrix removal, pre-concentration and analysis of 226 Ra using pre-packed columns coupled to a flow injection system and an ICP-MS was developed. Full instrumental control of both the ICP-MS and the flow injection system provided automatic integration of the transient signals. The flow injection system was programmed to control column conditioning, sample loading, column rinsing, analyte elution and column cleaning operations employing appropriate solutions. The application of this system to the 226 Ra analysis of an industrial liquid effluent was demonstrated. Using this particular instrument together with pre-concentration and matrix removal procedures, a limit of detection of 5.4 fg L −1 (2 mBq L −1 ) and a method detection limit of 16.2 fg L −1 (6 mBq L −1 ) were achieved for the measurement of 226 Ra using a 25 mL sample volume. Total time for sample handling and analysis is approximately 10 minutes. The concentration of 226 Ra in a discharged effluent sample was 0.73 pg L −1 (27 mBq L −1 ), which is in good agreement with the value of 0.81 pg L −1 (30 mBq L −1 ) measured using conventional alpha counting techniques." @default.
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• W2114958512 date "2015-11-01" @default.
• W2114958512 modified "2023-09-26" @default.
• W2114958512 title "Continuous online determination of ²²⁶Ra in liquid effluents using automated column chromatography-ICP-MS" @default.
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• W2114958512 doi "https://doi.org/10.1139/cjc-2015-0247" @default.
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