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W2115421738 abstract "Acrylamide detection still represents one of the hottest topics in food chemistry. Solid phase cleanup coupled to liquid chromatography separation and tandem mass spectrometry detection along with GC-MS detection are nowadays the gold standard procedure for acrylamide quantitation thanks to high reproducibility, good recovery, and low relative standard deviation. High-resolution mass spectrometry (HRMS) is particularly suitable for the detection of low molecular weight amides, and it can provide some analytical advantages over other MS techniques. In this paper a liquid chromatography (LC) method for acrylamide determination using HRMS detection was developed and compared to LC coupled to tandem mass spectrometry. The procedure applied a simplified extraction, no cleanup steps, and a 4 min chromatography. It proved to be solid and robust with an acrylamide mass accuracy of 0.7 ppm, a limit of detection of 2.65 ppb, and a limit of quantitation of 5 ppb. The method was tested on four acrylamide-containing foods: cookies, French fries, ground coffee, and brewed coffee. Results were perfectly in line with those obtained by LC-MS/MS." @default.
W2115421738 created "2016-06-24" @default.
W2115421738 creator A5008743211 @default.
W2115421738 creator A5046190544 @default.
W2115421738 creator A5053060196 @default.
W2115421738 date "2013-12-26" @default.
W2115421738 modified "2023-09-26" @default.
W2115421738 title "Quantitation of Acrylamide in Foods by High-Resolution Mass Spectrometry" @default.
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W2115421738 doi "https://doi.org/10.1021/jf404205b" @default.
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