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- W2116486145 abstract "Abstract A highly-efficient and practical method for the formation of ynones from a variety of acyl chlorides and terminal alkynes catalyzed by a nanosized MCM-41 anchored palladium bipyridyl complex is described herein. Aroyl, heteroaroyl, and alkyl acyl chlorides were easily coupled with terminal alkynes, giving good to high isolated yields in the presence of a very low catalyst loading (0.002–0.1 mol % Pd) in Et3N or diisopropylethylamine at 50 °C. Furthermore, the reaction scale was up to 150 mmol for a single batch reaction, providing the potential for practically synthetic application. After centrifugation, the supported catalyst was able to be recycled and reused several times with only a slight decrease in activity." @default.
- W2116486145 created "2016-06-24" @default.
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- W2116486145 date "2010-03-23" @default.
- W2116486145 modified "2023-09-26" @default.
- W2116486145 title "ChemInform Abstract: Highly-Efficient and Recyclable Nanosized MCM-41 Anchored Palladium Bipyridyl Complex-Catalyzed Coupling of Acyl Chlorides and Terminal Alkynes for the Formation of Ynones." @default.
- W2116486145 cites W2950651592 @default.
- W2116486145 doi "https://doi.org/10.1002/chin.201012077" @default.
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