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- W2116500238 abstract "A novel acetylated anhydroglucose oligomer (AGU-oligomer), prepared by acid catalyzed transglycosidation of potato starch triacetate and ethylene glycol, was used as a multifunctional coinitiator for the ring-opening polymerization of ε-caprolactone (ε-CL). The polymers were synthesized using different weight ratios of the starting materials and were characterized by NMR, SEC, and MALLS. The results confirmed the expected P(AGU/CL) polymer structure, namely a ‘comb-like’ graft-copolymer having the AGU oligomer as backbone with PCL grafts of variable chain lengths (LCL = 4–21). Thermal and mechanical properties of graft-copolymers with different ε-CL block lengths were examined. By changing the graft length, crystallinity was controlled and amorphous polymers were obtained with AGU-oligomer contents higher than 50 wt %. The tensile properties varied with the composition and a copolymer having 40 wt % of AGU-oligomer behaved like soft elastomer, showing high elongation at break. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 100: 1633–1641, 2006" @default.
- W2116500238 created "2016-06-24" @default.
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- W2116500238 date "2006-01-01" @default.
- W2116500238 modified "2023-09-27" @default.
- W2116500238 title "Poly(ɛ-caprolactone)-grafted acetylated anhydroglucose oligomer by ring-opening polymerization—Synthesis and characterization" @default.
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- W2116500238 doi "https://doi.org/10.1002/app.23697" @default.
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