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- W2116571289 abstract "Die Synthesen der aminoacylierten 5′-O-(4-Methoxytrityl)ribonucleoside des Adenosins (1), Guanosins (9), Cytidins (31), Uridins (17) und 5,6-Dihydrouridins (23) wurden optimiert und diese Verbindungen (4, 12, 33, 18 und 24) mit tert-Butyldimethylsilylchlorid silyliert. Die entsprechenden 2′- bzw. 3′-Mono-O- und 2′,3′-Bis-O-(tert-butyldimethylsilyl)-Derivate wurden durch Kombination von chromatographischen Methoden und fraktionierenden Kristallisationsverfahren in präparativem Maßstab gewonnen. Ihre Charakterisierung erfolgte durch UV- und 13C-NMR-Spektren. Nucleosides, XXXVII1) Synthesis and Properties of 2′-O- and 3′-O-(tert-Butyldimethylsilyl)-5′-O-(4-methoxytrityl)- and 2′,3′-Bis(O-tert-butyldimethylsilyl)ribonucleosides — Starting Materials for Oligoribonucleotide Syntheses The synthesis of aminoacylated 5′-O-(4-methoxytrityl)ribonucleosides of adenosine (1), guanosine (9), cytidine (31), uridine (17), and 5,6-dihydrouridine (23) have been optimized and these compounds (4, 12, 33, 18 and 24) silylated by tert-butyldimethylsilyl chloride. The corresponding 2′-and 3′-mono-O- as well as 2′,3′-bis-O-(tert-butyldimethylsilyl) derivatives have been isolated by combination of chromatographical methods and fractional crystallization procedures in preparative scale. The characterization of the newly synthesized compounds was achieved by UV and 13C-NMR spectra." @default.
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- W2116571289 date "1981-09-21" @default.
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- W2116571289 title "Nucleoside, XXXVII. Synthese und Eigenschaften von 2′-O- und 3′-O-(tert-Butyldi-methylsilyl)-5′-O-(4-methoxytrityl)- sowie 2′,3′-Bis-O-(tert-butyl-dimethylsilyl)ribonucleosiden — Ausgangssubstanzen für Oligoribonucleotid-Synthesen" @default.
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- W2116571289 doi "https://doi.org/10.1002/jlac.198119810907" @default.
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