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- W2116629757 abstract "New complexes with thiosemicarbazone derivative and 3, 4-dihydrocinnamic acid were prepared and characterized by elemental analysis, determination of metal, IR, 1 H NMR, electronic spectroscopy and magnetic measurements. The thiosemicarbazone derivative forms bidentate ligand complexes of the general formula, [M(Thz)(Caf)] where Thz = 4-formyl- acetanilide thiosemicarbazone, Caf = 3,4-dihydrocinnamic acid and M=Mn 2+ , Fe 2+ , Co 2+ , Ni 2+ , Cu 2+ , Zn 2+ , Cd 2+ and Pb 2+ . The IR and 1 H NMR spectra indicates that the (Thz) was coordinated with the metal ions through the N and S atoms and the (Caf) was negatively charged bidentat ligand and was coordinated with the metal ions through the two O atoms. Electronic spectra and magnetic susceptibility measurements of the solid complexes indicates the tetrahedral geometry around the Mn 2+ , Fe 2+ , Co 2+ , Ni 2+ , Zn 2+ , Cd 2+ and irregular tetrahedral geometry around Pb 2+ ion while the Cu 2+ complex has squar planer geometry." @default.
- W2116629757 created "2016-06-24" @default.
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- W2116629757 date "2010-01-01" @default.
- W2116629757 modified "2023-10-17" @default.
- W2116629757 title "Synthesis, Spectral and Magnetic Studies of Newly Mixed-Ligand Complexes of 4-Formyl-Acetanilide Thiosemicarbazone and 3,4-Dihydrocinnamic Acid with Some Metal Ions" @default.
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- W2116629757 doi "https://doi.org/10.1155/2010/307842" @default.
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