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- W2116725107 abstract "Abstract Even though 2,2′‐diiodo‐ and 2,2′‐dibromobiaryls represent accomplished precursors for heterofluorenes and other extended π‐conjugated systems, their preparation still remains nontrivial when structural diversity of the biaryl backbone is required. Herein, we report a convenient method for the preparation of various 2,2′‐diiodobiaryls from 2‐iodobiaryls via cyclic diaryliodonium intermediates. An iodinative ring‐opening of the diaryliodonium salts, mediated by a copper/diamine catalyst system, is able to afford the corresponding 2,2′‐diiodobiaryls under mild conditions. The versatility of this two‐step approach is demonstrated by the preparation of hitherto unexplored tetraiodoteraryls and their conversion into ladder‐type π‐conjugated systems." @default.
- W2116725107 created "2016-06-24" @default.
- W2116725107 creator A5024512544 @default.
- W2116725107 creator A5089549225 @default.
- W2116725107 date "2015-06-08" @default.
- W2116725107 modified "2023-10-18" @default.
- W2116725107 title "Conversion of 2-Iodobiaryls into 2,2′-Diiodobiaryls via Oxidation-Iodination Sequences: A Versatile Route to Ladder-Type Heterofluorenes" @default.
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- W2116725107 doi "https://doi.org/10.1002/anie.201503134" @default.
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