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- W2116744806 abstract "The structure factors for the 111 and the “forbidden” 222 reflections of germanium are consistently determined by combining two independent electron diffraction measurements: 1. the critical voltage Ec = (908.5 ± 6.4) kV for the 333 reflection and 2. the rocking curves in convergent-beam diffraction patterns taken at the 111 and 222 Bragg settings with incident electrons of 100 kV. The values obtained for these factors without thermal vibrations are F = −155.74 ± 0.07 and F = 1.24 ± 0.32. These correspond to the atomic scattering factor f111 = 27.53 ± 0.01 and the anti-centrosymmetric component of f222, f = −0.16 ± 0.04, respectively. The mean value of f111 is in good agreement with earlier X-ray measurements and its percentage error, 0.04%, is much smaller than other published values.Die Rontgenstrahl-Strukturfaktoren fur die 111- und die „verbotenen” 222-Reflexe von Germanium werden konsistent durch zwei unabhangige Elektronenbeugungsmessungen bestimmt: 1. durch die kritische Spannung Ec = (908,5 ± 6,4) kV fur den 333-Reflex und 2. durch die Rocking-Kurven im Beugungsdiagramm im konvergenten Bundel bei Anregungen der 111- und 222-Reflexe mit einer Strahlspannung von 100 kV. Die erhaltenen Werte fur diese Faktoren ohne Temperaturfaktor sind F = −155,74 ± 0,07 und F = = 1,24 ± 0,32. Diese entsprechen der Atomformamplitude von f111 = 27,53 ± 0,01 und dem antisymmetrischen Bestandteil von f222, f = −0,16 ± 0,04. Der Mittelwert von f111 ist in guter Ubereinstimmung mit den Ergebnissen fruherer Rontgenmessungen und die Genauigkeit von 0,04% ist viel besser als andere berichtete Werte." @default.
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- W2116744806 date "1976-12-16" @default.
- W2116744806 modified "2023-09-26" @default.
- W2116744806 title "Determination of structure factors of germanium by the critical-voltage and convergent-beam diffraction methods" @default.
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- W2116744806 doi "https://doi.org/10.1002/pssa.2210380205" @default.
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