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- W2116895536 abstract "Trifluoromethyl- or difluoromethylene-substituted alkyl radicals (CF3C or CF2C) and trifluoromethyl- substituted alkenyl radicals (CF3CC) cyclize effectively intramolecularly to allow the synthesis of fluorine- substituted cyclic compounds. Radical reactions of thiocarbonylimidazolide derivatives (7a,b, 13a–d, 14e,f) gave CF3-substituted cyclopentane derivatives (22a, 25a–d) or cyclohexane derivatives (22b, 26e,f) via 5- or 6-exo selective cyclization. CF3-substituted cyclopentene derivatives (27a,b) or cyclohexene derivatives (27c) were also obtained from alkenyl iodides (17a–c) via radical cyclization. Cyclopentane derivatives (29a–f, 31) containing the CF2CO2Et group were synthesized by Reformatsky reaction and radical cyclization." @default.
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- W2116895536 date "1993-11-01" @default.
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- W2116895536 title "Free-radical approach to the synthesis of fluorine-substituted cyclic compounds. Cyclization reactions of trifluoromethyl-and difluoromethylene-substituted carbon radicals" @default.
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- W2116895536 doi "https://doi.org/10.1016/s0022-1139(00)80477-7" @default.
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