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- W2117535211 abstract "Thionation of pentacyclo[5.4.0.0 2 , 6 .0 3 . 1 0 .0 5 , 8 ]undecane-8-one (2) with P 2 S 5 in pyridine afforded the corresponding thione 7 in good yield (70%). In contrast to this result, the P 2 S 5 promoted thionation of pentacyclo[5.4.0.0 2 , 6 .0 3 . 1 0 .0 5 , 8 ]undecane -8,11-dione (1) did not afford the expected dithiocarbonyl derivative. Alternatively, reaction of methanolic 1 with H 2 S(g)/HCl(g) led to the thiocarbonyl derivatives 8 and 9. At longer reaction times (3-5 h), this reaction afforded two unexpected products 10 and 11, both of which are 3,5-disubstituted-4-thiahexacyclo[5.4.1.0 2 , 6 .0 3 , 1 0 .0 5 , 9 ]-dodecanes." @default.
- W2117535211 created "2016-06-24" @default.
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- W2117535211 date "2010-05-19" @default.
- W2117535211 modified "2023-10-14" @default.
- W2117535211 title "ChemInform Abstract: First Synthesis of Thiocarbonyl Derivatives of Cage Ketones." @default.
- W2117535211 cites W2951009171 @default.
- W2117535211 doi "https://doi.org/10.1002/chin.200243096" @default.
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