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- W2118701802 abstract "Abstract The formation of four differently protected 4‐deoxy‐D‐lyxo‐hexose derivatives 7, 8, 12, and 14 is described. In the first procedure, a nucleophilic displacement of the allylic mesylate 4 by hydride was combined with a highly stereoselective osmylation of olefin 6 to afford diol 7. In the second radical procedure, tributyl tin hydride was substituted by the cheap and environmentally friendly hypophosphorous acid as a hydrogen donor in the reduction of xanthate 13 to 4‐deoxy lyxo‐hexose 14. Keywords: 4‐Deoxy‐D‐lyxo‐hexoseLiAlH4 reduction of allylic mesylateStereoselective cis‐hydroxylationHypophosphorous acidDeoxygenation Dedicated to Prof. Siegfried Blechert on the occasion of his 60th birthday." @default.
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- W2118701802 date "2006-06-01" @default.
- W2118701802 modified "2023-09-30" @default.
- W2118701802 title "Two Efficient Syntheses of Protected 4‐Deoxy‐<scp>D</scp>‐lyxo‐hexose (4‐Desoxy‐<scp>D</scp>‐mannose)" @default.
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