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- W2120357054 abstract "Riluzole is a benzothiazole derivative, used to treat amyotrophic lateral sclerosis. During the process development of riluzole, nine unknown peaks (related compounds/impurities) were observed in HPLC analysis in the range of 0.05 to 0.15%. These impurity samples were analyzed by LC-MS and the respective peaks were identified at m/z 177, 177, 177, 234, 234, 312, 255, 396 and 333. Among the nine impurities, six impurities were identified as process-related impurities and the remaining three impurities were assigned to the starting material and its isomers. The six process-related impurities were synthesized and characterized based on their spectral data (IR, NMR and MS)." @default.
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- W2120357054 date "2008-10-02" @default.
- W2120357054 modified "2023-10-17" @default.
- W2120357054 title "Synthesis and spectral characterization of related compounds of riluzole, an amyotrophic lateral sclerosis drug substance" @default.
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- W2120357054 doi "https://doi.org/10.3998/ark.5550190.0009.e12" @default.
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