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- W2121567211 abstract "Stereoselective syntheses of tricyclo[5.3.0.0(3,8)]decane 22 and tricyclo[6.3.0.0(3,9)]undecane 26, the basic skeletons of copaborneol and longiborneol, were achieved by the intramolecular double Michael reactions of 2-cyclopenten-1-ones 15-17. The substrates were prepared starting with tricyclo[5.2.1.0(2,6)]deca-4,8-dien-3-one (6). The intramolecular double Michael reactions were carried out under three different conditions: TMSCl-Et(3)N-ZnCl(2), TMSI-(TMS)(2)NH, and Bu(2)BOTf-(TMS)(2)NH. The framework 26 of longiborneol was constructed in good yields using the latter two reagent systems." @default.
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- W2121567211 date "2010-08-04" @default.
- W2121567211 modified "2023-09-25" @default.
- W2121567211 title "ChemInform Abstract: Stereoselective Construction of Copaborneol and Longiborneol Frameworks by Intramolecular Double Michael Reaction." @default.
- W2121567211 cites W2949516537 @default.
- W2121567211 doi "https://doi.org/10.1002/chin.199702160" @default.
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