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- W2122190310 abstract "The preparation and a preliminary chromatographic evaluation of a novel polymeric chiral stationary phase (CSP) derived from (1R;2R)-diaminocyclohexane (DACH) are presented. A radical copolymerization process has been employed to generate a silica-based chiral sorbent, showing considerable high chemical and thermal stability and stereoselectivity toward racemic compounds capable of H-bonding (3-hydroxy-benzodiazepin-2-ones, chlorthalidone, atropoisomeric sulfur compounds, etc.); in the present paper we present the investigation on the resolution of racemic dihydroxy biarylic atropoisomers; the effects of eluent composition and of temperature on the separation ability of the CSP have been studied in order to elucidate the recognition mechanism operating in these chiral separations. © 1992 Wiley-Liss, Inc." @default.
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- W2122190310 date "1992-01-01" @default.
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- W2122190310 title "HPLC resolution of atropoisomeric compounds on a csp derived from (1R;2R)-diaminocyclohexane: Thermodynamic data from variable temperature chromatography" @default.
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- W2122190310 doi "https://doi.org/10.1002/chir.530040609" @default.
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