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- W2122800199 abstract "An efficient, general procedure for reductive monoalkyl- ation of amines and amine derivatives with aldehydes is reported. Treatment of aldehydes with primary amines, secondary amines, O- trimethylsilylhydroxylamine, and N,N-dimethylhydrazine in lithi- um perchlorate/diethyl ether and trimethylsilyl chloride, followed by BH3·NEt3 reduction, and straightforward workup afforded sec- ondary amines, tertiary amines, N-substituted hydroxylamines, and hydrazines, respectively. Reductive alkylation of a-amino esters with aldehydes afforded the corresponding N-monoalkylated a- amino esters selectively." @default.
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- W2122800199 date "2005-08-09" @default.
- W2122800199 modified "2023-10-16" @default.
- W2122800199 title "A General One-Pot, Three-Component Mono N-Alkylation of Amines and Amine Derivatives in Lithium Perchlorate/Diethyl Ether Solution." @default.
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- W2122800199 doi "https://doi.org/10.1002/chin.200532061" @default.
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