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- W2123014026 abstract "The reaction of (CH3)2Si[Cp′Fe(CO)2]2 with elemental sulfur in refluxing toluene resulted in the formation of two new iron-sulfur cluster compounds. Prolonged crystallisation from CH2Cl2-hexane mixtures of one of these compounds resulted in crystals of the title compound. An X-ray diffraction study revealed that two (CH3)2SiCp′2Fe2 units are connected to a central Fe(III) ion via four disulfido ligands and a tetrasulfido ligand. This iron atom is octahedrally coordinated by six sulfur atoms. Of the six Fe(III)S distances four are close to 2.30 Å and the other two are about 2.20 Å. In both the (Ch3)2SiCp′2Fe2 units each iron atom is coordinated to three sulfur atoms and one Cp ring. This results in twelve FeS distances: six of them are in a narrow range from 2.165 to 2.184 Å, whereas the other six vary from 2.240 to 2.286 Å. The FeFe distances are 2.561 and 2.581 Å. The SS distances range from 2.041 to 2.073 Å. The FeCl distances in the FeCl4− ion, centred around 2.16 Å, show the presence of Fe(III) in this ion." @default.
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- W2123014026 date "1994-02-01" @default.
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- W2123014026 title "Two silicon-bridged cyclopentadienyl Fe2S4 cluster units connected through an Fe(III)S6 unit. Crystal and molecular structure of [((CH3)2SiCp′2)2Fe5(μ3-S2)2(μ4-S2)2(μ4-S4)]FeCl4" @default.
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- W2123014026 doi "https://doi.org/10.1016/0020-1693(93)03719-q" @default.
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