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- W2123420006 abstract "Abstract The molecular steps involved in the self‐assembly of Cu 3 (BTC) 2 (BTC=1,3,5‐benzenetricarboxylic acid) metal–organic frameworks that enclose Keggin‐type H 3 PW 12 O 40 heteropolyacid molecules were unraveled by using solution 17 O, 31 P, and 183 W NMR spectroscopy, small‐angle X‐ray scattering, near‐IR spectroscopy, and dynamic light scattering. In aqueous solution, complexation of Cu 2+ ions with Keggin‐type heteropolyacids was observed. Cu 2+ ions are arranged around the Keggin structure so that linking through benzenetricarboxylate groups results in the formation of the Cu 3 (BTC) 2 MOF structure HKUST‐1. This is a unique instance in which a templating mechanism that relies on specific molecular‐level matching and leads to explicit nanoscale building units can be observed in situ during formation of the synthetic nanoporous material." @default.
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- W2123420006 date "2010-03-26" @default.
- W2123420006 modified "2023-10-18" @default.
- W2123420006 title "Direct Observation of Molecular-Level Template Action Leading to Self-Assembly of a Porous Framework" @default.
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- W2123420006 doi "https://doi.org/10.1002/chem.200903239" @default.
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