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- W2123673886 abstract "A method has been developed for the determination of traces of boron in graphite powder. The graphite powder was made into a paste using Na2CO3 solution (flux). The paste form of graphite powder was fused in a muffle furnace and was mixed in a glycerol solution. The flux was separated from the glycerol solution as a solid residue by heating over a water bath. The boron present in the glycerol solution was measured by ICP-OES. Compared to conventional Na2CO3 fusion, the amount of flux and fusion time were reduced by a factor of 32 and 8, respectively. Due to the extraction of boron from the flux into glycerol solution, the preconcentration was increased by a factor of 200. The separation of flux was >92% with the recovery of analyte in the range of 92–96%. The detection limit was found to be 90 ng g−1." @default.
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- W2123673886 date "2013-01-01" @default.
- W2123673886 modified "2023-09-27" @default.
- W2123673886 title "Determination of trace levels of boron in graphite powder by inductively coupled plasma-optical emission spectrometry (ICP-OES)" @default.
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- W2123673886 doi "https://doi.org/10.1039/c3ay41255e" @default.
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