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- W2123770383 abstract "Abstract A novel method is proposed to access to new poly(α‐amino‐ε‐caprolactone‐ co ‐ε‐caprolactone) using poly(α‐iodo‐ε‐caprolactone‐ co ‐ε‐caprolactone) as polymeric substrate. First, ring‐opening (co)polymerizations of α‐iodo‐ε‐caprolactone (αIεCL) with ε‐caprolactone (εCL) are performed using tin 2‐ethylhexanoate (Sn(Oct) 2 ) as catalyst. (Co)polymers are fully characterized by 1 H NMR, 13 C NMR, FTIR, SEC, DSC, and TGA. Then, these iodinated polyesters are used as polymeric substrates to access to poly(α‐amino‐ε‐caprolactone‐ co ‐ε‐caprolactone) by two different strategies. The first one is the reaction of poly(αIεCL‐ co ‐εCL) with ammonia, the second one is the reduction of poly(αN 3 εCL‐ co ‐εCL) by hydrogenolysis. This poly(α‐amino‐ε‐caprolactone‐ co ‐ε‐caprolactone) ( F αNH2εCL < 0.1) opens the way to new cationic and water‐soluble PCL‐based degradable polyesters. © 2009 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 47: 6104–6115, 2009" @default.
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- W2123770383 date "2009-10-07" @default.
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- W2123770383 title "Aminated PCL-based copolymers by chemical modification of poly(α-iodo-ε-caprolactone-<i>co</i> -ε-caprolactone)" @default.
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- W2123770383 doi "https://doi.org/10.1002/pola.23652" @default.
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