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• W2124430669 abstract "The monotopic crown ether ligands (5 and 6) and their sodium perchlorate complexes (5a and 6a) have been synthesized. The crystal structure of (5) has been determined, which contains 1 mol of water molecule. Compound (5) crystallizes in the monoclinic space group C 2/ c with a =39.324(8), b =8.011(1), c =16.877(4) Å, β =107.61(2)°, V =5067.5(2) Å 3 , Z =8 and D calc =1.289 g m −3 . The relative macrocyclic inner hole size, estimated as twice the mean distance of the donor atoms from their centroid is approximately 1.68 Å. The phenazone and benzo crown ether precursors about C N imine bond are in anti ( E ) configuration. The C N imine bond length and C N–C bond angle are 1.270(3) Å and 120.4(2)°, respectively. Compounds (6) and (6a) are in phenol-imine forms as supported by 1 H-NMR and UV–visible data." @default.
• W2124430669 created "2016-06-24" @default.
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• W2124430669 date "2001-10-01" @default.
• W2124430669 modified "2023-10-18" @default.
• W2124430669 title "Synthesis, complex formation, spectral and crystallographic investigations of new crown ethers containing recognition site for sodium. Part V" @default.
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• W2124430669 doi "https://doi.org/10.1016/s0022-2860(01)00603-2" @default.
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