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- W2124606989 abstract "The strong correlation of melting behavior with the microstructure of original and zone-drawn isotactic polypropylene fibers was evaluated by microthermal analysis (micro-TA) combined with wide-angle X-ray diffraction analysis. The crystal structure of both the original and zone-drawn fibers was a monoclinic α-form with a ∼ 0.64 nm, b ∼ 2.03 nm, and c ∼ 0.65 nm. In contrast to the absence of any oriented polymer molecules in the original fiber, the polymer molecules in the zone-drawn fiber were extended and highly oriented in at least two different states; one arranged along the drawn axis and the other at 40° to the drawn axis. The micro-TA-derived melting points corresponded to these microstructural changes caused by the zone-drawing process and differed from the melting points obtained by differential scanning calorimetery. The micro-TA melting point of 140°C corresponded to the z-e-p melting point of the original fiber, being much lower than the conventional differential scanning calorimetery melting point of 163°C. As for the zone-drawn fiber, an increase of 19°C in the melting temperature revealed its high orientation level, and the appearance of three elevated melting peaks (161, 167, and 178°C) at the highest heating rate (1500°C/min) coincided with its several oriented states. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 100: 1306–1311, 2006" @default.
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- W2124606989 date "2006-01-01" @default.
- W2124606989 modified "2023-10-06" @default.
- W2124606989 title "Evaluation of the microstructure and melting behavior of drawn polypropylene fibers with a microthermal analyzer" @default.
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- W2124606989 doi "https://doi.org/10.1002/app.23412" @default.
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