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• W2124699296 startingPage "32" @default.
• W2124699296 abstract "Thermal reactions of Cp2Mo2(CO)4(μ-η2-C14H20) (1) with Fe3(CO)12 and Ru3(CO)12 produce [Cp2Mo2(CO)4](μ,μ3-η2,η2-C14H20)[Fe3(CO)9] (2) and [Cp2Mo2(CO)4](μ,μ3-η2,η3-C14H19)[(μ-H)Ru3(CO)9] (3-allyl), respectively, while treatments of 1 with Ru3(CO)10(NCMe)2 and Os3(CO)10(NCMe)2 afford [Cp2Mo2(CO)4](μ,μ3-η2,η3-C14H19)[(μ-H)Ru3(CO)9] (3-allenyl) and [Cp2Mo2(CO)4](μ,μ3-η2,η2-C14H20)[Os3(CO)10] (4), respectively. The allene moiety of 3-allenyl rearranges upon heating to give the allyl complex 3-allyl. Compound 1 reacts with Co2(CO)8 to produce [Cp2Mo2(CO)4](μ,μ-η2,η2-C14H20)[Co2(CO)6] (5) and the reaction of Os3(CO)10(μ3-η2-C14H20) with Co2(CO)8 affords [Os3(CO)10](μ3,μ-η2,η2-C14H20)[Co2(CO)6] (6). The new compounds 2–6 have been characterized by mass, IR and NMR spectroscopy. The crystal structure of 4 reveals a bridging and a semibridging carbonyl connected to the Os3 cluster." @default.
• W2124699296 created "2016-06-24" @default.
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• W2124699296 date "1999-10-01" @default.
• W2124699296 modified "2023-09-26" @default.
• W2124699296 title "Preparation of Mo, Co and iron group heterometallic clusters linked by cyclotetradeca-1,8-diyne ligand" @default.
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• W2124699296 doi "https://doi.org/10.1016/s0022-328x(99)00342-3" @default.
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