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- W2125881372 abstract "Synthesis o f clusters o f acicular MFI zeolites from porous silica layers strongly attached to stainless steel surfaces is reported. The porous silica layers are prepared by pyrolysis o f silicone rubber layers applied from solutions in ethylacetate or dimethylether. The surface area o f the silica is about 100 m2/g of silica, the pore volume about 0.13 m l/g o f silica. XPS spectra indicate the metal to be completely covered by the silica. The template solution is impregnated into the pore volume of the silica layer, after which the coated steel plate is treated hydrothermally for at least 18 hours at 170°C in a solution of silica in ammoniumhydroxide. The resulting MFI crystallites have been deposited on the surface o f the stainless steel as clusters o f about 1.5 |a.m consisting of small acicular crystallites. The density o f clusters depends on the thickness o f the initial silica layer. The X-ray pattern is that o f MFI and indicates some preferred orientation. The clusters are strongly adhering to the metal surface provided that grease and oxide layer have been completely removed by rinsing and polishing. The open structure o f the clusters o f zeolite crystallites leads to a large external surface area facilitating transport into the pore structure of the zeolites." @default.
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- W2125881372 date "1999-01-01" @default.
- W2125881372 modified "2023-09-23" @default.
- W2125881372 title "GROWTH OF ZEOLITES FIRMLY ATTACHED TO METAL SURFACES FOR USE IN CATALYSIS" @default.
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