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- W2126090835 abstract "A simple and time-efficient method, based on capillary zone electrophoresis, was developed for the simultaneous determina- tion of bromhexine (BMX) and amoxicillin (AMX) in pharmaceuti- cal formulations. The optimized electrophoretic conditions comprise 50 mM sodium phosphate plus 50 mM citric acid as running buffer (pH 3.0), cartridge temperature 25°C, hydrodynamic injection (5 s. at 0.5 psi), 30 kV separation voltage, and UV detection at 214 nm. The analytes were separated in less than 5 min. Formulation samples were processed by successive treatment with methanol, hydrochloric acid, filtering and dilution in the running buffer. Loperamide was used as internal standard for quantitation. A linear detection range of 10-85 μg/mL for BMX (R 2 = 0.997) and 250-2010 μg/mL for AMX (R 2 = 0.995) was observed, with LOD for BMX as low as 2 μg/mL. The developed method enabled high analyte recoveries (99-104%) and excellent run-to-run reproducibility. Moreover, it was successfully employed for the determination of BMX and AMX in several phar- maceutical formulations, demonstrating its applicability to the routine quality control." @default.
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- W2126090835 date "2011-06-01" @default.
- W2126090835 modified "2023-10-01" @default.
- W2126090835 title "Simultaneous Determination of Bromhexine and Amoxicillin in Pharmaceutical Formulations by Capillary Electrophoresis" @default.
- W2126090835 cites W2890227075 @default.
- W2126090835 doi "https://doi.org/10.29356/jmcs.v55i2.835" @default.
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