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- W2126924871 abstract "[92149-07-0] C14H12N2O2 (M.W. 240.26)InChI = 1S/C14H12N2O2/c1-17-11-5-7-15-13-9(11)3-4-10-12(18-2)6-8-16-14(10)13/h3-8H,1-2H3InChIKey = ZPGVCQYKXIQWTP-UHFFFAOYSA-N(reagent used as a chelating ligand for a variety of transition metal-catalyzed processes5-7, 11-14)Physical Data: (mp 209–210 °C).Solubility: soluble in methanol, N-methylpyrrolidinone, dimethylsulfoxide, acetone, 1,4-dioxane(aq), dichloromethane, chloroform, hot toluene.Analysis of Reagent Purity: 1H NMR, EA.Form Supplied in: tan to white solid. Small quantities are commercially available.Preparative Methods: from 4,7-dihydroxy-1,10-phenanthroline, chlorination with POCl3 or POCl3/PCl5, followed by nucleophilic aromatic substitution of the resulting 4,7-dichloride with NaOMe.5, 15Purification: dissolution in methanol and precipitation from H2O (pH <9). Recrystallization from hot toluene or benzene.Handling, Storage, and Precautions: 4,7-dimethoxy-1,10-phenanthroline is thermally stable and stable to oxidation. 1,10-Phenanthrolines readily absorb 1 equiv of water. Contact with skin, or eyes, or inhalation can cause irritation. This compound is harmful if swallowed. Wear proper protective apparel when working with this reagent." @default.
- W2126924871 created "2016-06-24" @default.
- W2126924871 creator A5070642346 @default.
- W2126924871 date "2008-09-15" @default.
- W2126924871 modified "2023-09-26" @default.
- W2126924871 title "1,10-Phenanthroline, 4,7-Dimethoxy" @default.
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- W2126924871 doi "https://doi.org/10.1002/047084289x.rn00918" @default.
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