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- W2127440379 abstract "The action of sodium azide on (dibromomethyl)pyrimidines 2a and 8a leads to the nitriles 3a and 9, whereas the 1-methyl derivatives 2b and 8b afford the geminal diazides 7 and 10. The nitriles 3a, b add another mole of azide to give the tetrazoles 4a, b. The palladium-catalyzed decomposition of azide 5, obtained from bromide 6 by treatment with sodium azide, yields nitrile 3a." @default.
- W2127440379 created "2016-06-24" @default.
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- W2127440379 date "1990-05-11" @default.
- W2127440379 modified "2023-10-16" @default.
- W2127440379 title "Synthesis and reactions of biginelli compounds, 3. Unexpected formation of nitriles from reactions of 6-(dibromomethyl)-1,2,3,4-tetrahydro-2-oxo-5-pyrimidinecarboxylates with sodium azide" @default.
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- W2127440379 doi "https://doi.org/10.1002/jlac.199019900196" @default.
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