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• W2127966870 startingPage "14624" @default.
• W2127966870 abstract "Abstract Mesoporous graphitic carbon nitride (mpg‐C 3 N 4 ) was found to be an efficient heterogeneous photocatalyst for the metal‐free radical cyclization of 2‐bromo‐1,3‐dicarbonyl compounds. Reactions leading to functionalized cyclopentanes proceed under mild conditions and can be conducted in a continuous flow photoreactor. Compared to the batch reaction, the use of a continuous flow reactor resulted in a significant reduction in reaction time (complete conversion of 0.04 mmol of substrate in a batch was achieved after 4 h, whereas in a flow reactor the same amount of substrate was fully converted into a product within 40 min). Mechanistic studies of the reaction showed that THF plays not only the role of solvent, but is also a crucial hydrogen and electron donor." @default.
• W2127966870 created "2016-06-24" @default.
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• W2127966870 date "2014-09-24" @default.
• W2127966870 modified "2023-09-30" @default.
• W2127966870 title "THF: An Efficient Electron Donor in Continuous Flow Radical Cyclization Photocatalyzed by Graphitic Carbon Nitride" @default.
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• W2127966870 doi "https://doi.org/10.1002/chem.201404440" @default.
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• W2127966870 hasPublicationYear "2014" @default.
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