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- W2129124726 abstract "Die als Zwischenprodukte im Rahmen einer Moenocinol-Synthese vorgesehenen Verbindungen 15 und 16 konnten durch Grob-Fragmentierung aus 14 bzw. 17 nicht erhalten werden. Stattdessen reagierte 17 mit Natriummethanolat zu 34, 36 und 38, und aus 14 entstand unter Baseneinwirkung das Oxetan 43. Die Modellverbindungen 27 und 30 gingen die erwünschte Fragmentierungsreaktion ein. Außerdem wird die Spaltung des Oxetans 32 mit Zirconocen beschrieben. On the Synthesis of the C25-Alcohol Moenocinol. – Studies on the Fragmentation Behaviour of Cyclic β-Ketotosylates and β-Hydroxytosylates Compounds 15 and 16, designated as intermediates in a moenocinol synthesis, could not be obtained by Grob fragmentation of 14 and 17, respectively. 17 furnished 34, 36, and 38 on treatment with sodium methoxide, and 14 gave the oxetane 43 under basic conditions. The expected fragmentation reactions could be achieved with the model compounds 27 and 30. In addition, cleavage of the oxetane 32 with zirconocene is reported." @default.
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- W2129124726 date "1985-04-15" @default.
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- W2129124726 title "Zur Synthese des C25-Alkohols Moenocinol Fragmentierungsversuche an cyclischen β-Ketotosylaten und β-Hydroxytosylaten" @default.
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- W2129124726 doi "https://doi.org/10.1002/jlac.198519850419" @default.
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