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• W2129332603 abstract "[29934-17-6] and [78655-99-9] C36H66Cl2P2Pd (MW 738.18) InChI = 1S/2C18H33P.2ClH.Pd/c2*1-4-10-16(11-5-1)19(17-12-6-2-7-13-17)18-14-8-3-9-15-18;;;/h2*16-18H,1-15H2;2*1H;/q;;;;+2/p-2 InChIKey = VUYVXCJTTQJVKJ-UHFFFAOYSA-L InChI = 1/2C18H33P.2ClH.Pd/c2*1-4-10-16(11-5-1)19(17-12-6-2-7-13-17)18-14-8-3-9-15-18;;;/h2*16-18H,1-15H2;2*1H;/q;;;;+2/p-2/f2C18H33P.2Cl.Pd/h;;2*1h;/q;;2*-1;m InChIKey = VUYVXCJTTQJVKJ-RNQHKKAHCS (reagent use as catalyst precursor in a wide array of carbon–carbon and carbon–heteroatom bond forming reactions) Physical Data: mp 297–300 °C (dec).1 Solubility: moderately soluble in dichloromethane and chloroform; sparingly soluble in benzene and toluene; insoluble in water, alcohols, acetone, diethyl ether, and hexanes. Form Supplied in: pale yellow microcrystalline powder. Analysis of Reagent Purity: 1H NMR (300 MHz, CDCl3) δ = 1.0–2.7 (m); 31P NMR (121.5 MHz, CDCl3) δ = 25.4 (s);13C NMR (75 MHz, CDCl3) δ = 27.3 (s), 28.3 (virtual triplet, 2JC−P + 4JC-P =10.7 Hz), 30.3 (s), 32.5 (virtual triplet, 1JC-P + 3JC-P =20.0 Hz).1 Purification: may be washed with water, ethanol, and diethyl ether, and then dried under vacuum. Can be recrystallized with minor losses from boiling o-dichlorobenzene. Handling, Storage and Precautions: air-stable in the solid state (for years) and in solution (at least several days)." @default.
• W2129332603 created "2016-06-24" @default.
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• W2129332603 date "2008-09-15" @default.
• W2129332603 modified "2023-09-28" @default.
• W2129332603 title "Dichlorobis(tricyclohexylphosphine)palladium" @default.
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• W2129332603 doi "https://doi.org/10.1002/047084289x.rn00850" @default.
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