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- W2129565284 abstract "Newly designed PS/PEO alternating branched polymacromonomers have been obtained by polycondensation of alpha-dicarboxy-functionalized polystyrene and alpha-dihydroxy-functionalized polyethyleneoxide. 4-[3,5-Bis(methoxycarbonyl)phenoxymethyl]benzyl bromide was used as atom-transfer radical polymerization (ATRP) initiator for the synthesis of alpha-dicarboxy functionalized polystyrenes. These macromonomers possess low polydispersities and molecular weights in the range of 7000 to 100,000, as proved by gel permeation chromatography (GPC) and 1H NMR. Alpha-dihydroxy functionalized polyethyleneoxide (PEO) was synthesized by treatment of monofunctionalized PEO with 3,5-bis(benzyloxy)benzoyl chloride. Polycondensation of the alpha-dicarboxy PS with the alpha-dihydroxy PEO in solution or in bulk resulted in alternating PS/PEO polymacromonomers, which were effectively purified from the unreacted macromonomers and characterized by using 1H NMR, GPC, thermal analysis, and optical microscopy. Light-scattering measurements in organic solvents like THF or dioxane have shown that these polymacromonomers form stable micelles." @default.
- W2129565284 created "2016-06-24" @default.
- W2129565284 creator A5042738350 @default.
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- W2129565284 date "2002-01-18" @default.
- W2129565284 modified "2023-10-17" @default.
- W2129565284 title "Synthesis of Alternating Polystyrene/Poly(ethyleneoxide) Branched Polymacromonomers" @default.
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- W2129565284 doi "https://doi.org/10.1002/1521-3765(20020118)8:2<467::aid-chem467>3.0.co;2-1" @default.
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