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- W2129996036 abstract "A highly efficient and mild procedure for the trimethylsilylation of a wide variety of alcohols, including primary, benzylic, secondary, hindered secondary, tertiary, phenols, and oximes with hexamethyldisilazane (HMDS), using Al(H 2 PO 4 ) 3 as a recyclable heterogeneous catalyst at room temperature in a few minutes with excellent yields under solvent-free conditions is described.Key words: trimethylsilylation, hexamethyldisilazane, aluminum tris(dihydrogen phosphate) [Al(H 2 PO 4 ) 3 ], solvent-free, hydroxyl groups." @default.
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- W2129996036 date "2008-08-01" @default.
- W2129996036 modified "2023-10-18" @default.
- W2129996036 title "An efficient method for the silylation of hydroxyl groups with hexamethyldisilazane (HMDS) catalyzed by aluminum tris(dihydrogen phosphate) under solvent-free and ambient conditions" @default.
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- W2129996036 doi "https://doi.org/10.1139/v08-086" @default.
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