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• W2130483451 endingPage "1573" @default.
• W2130483451 startingPage "1570" @default.
• W2130483451 abstract "The characterizations of the anhydrate (A-form), monohydrate (B1-form), and dihydrate (B2-form) of CS-834 were investigated by powder X-ray diffraction, differential scanning calorimetry (DSC), thermogravimetry-differential thermal analysis (TG-DTA), infrared spectroscopy, and Karl Fischer moisture titration. The typical DSC curve of the B2-form showed five endothermic peaks at 35.0, 46.4, 56.2, 99.2, and 190.4 degrees C and an exothermic peak at 123.4 degrees C. In TG-DTA analysis, the three peaks at 35.0, 46.4, and 56.2 degrees C had a total weight loss of 7.3%, corresponding to the release of two water molecules. From morphological observation under thermomicroscopy, the endothermic peak at 99.2 degrees C was attributed to the melting of the dehydrous crystals (B0-form) and the exothermic peak at 123.4 degrees C to the recrystallization to the A-form crystals. The endothermic peak at 190.4 degrees C was due to the melting of the A-form crystals. After incubation for 6.0 h at 35, 50, 60, and 80 degrees C, the powder X-ray diffraction patterns of the B2-form indicated that it was converted into the A-form via the B1-form and B0-form. Thus CS-834 exists in homologous hydrous crystal forms in multiple-phase transformations with the dehydration of two water molecules." @default.
• W2130483451 created "2016-06-24" @default.
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• W2130483451 date "2002-01-01" @default.
• W2130483451 modified "2023-10-02" @default.
• W2130483451 title "Physicochemical Analyses of Phase Transition and Dehydration Processes of a New Oral 1.BETA.-Methylcarbapenem Antibiotic Agent, CS-834." @default.
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• W2130483451 doi "https://doi.org/10.1248/cpb.50.1570" @default.
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