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- W2131032741 abstract "Abstract Reaction of the sodium salts of RC(S) NHP(S)(O‐i‐Pr) 2 (R = Ph, HL I ; PhNH, HL II ; 2‐MeC 6 H 4 NH, HL III ; 2,6‐Me 2 C 6 H 3 NH, HL IV ; 2,4,6‐Me 3 C 6 H 2 NH, HL V ) or Z[NHC(S)NHP(S)(O‐i‐Pr) 2 ] 2 (Z = o‐C 6 H 4 , H 2 L VI ; 1,2‐CH 2 CH 2 , H 2 L VII ) with PPh 4 Br in 96% aqueous EtOH leads to the compounds of formulae PPh 4 L I–V and (PPh 4 ) 2 L VI,VII . Compounds obtained were investigated by 1 H and 31 P{ 1 H} NMR spectroscopy, ES mass spectrometry, and microanalysis. Recrystallization of PPh 4 L I from an aqueous EtOH solution (1:1, v/v) leads to the formation of PhC(S)NHP(O)(O‐i‐Pr) 2 ( HQ ). The crystal structure of HQ reveals to be a polymorph to the previously reported structure. © 2010 Wiley Periodicals, Inc. Heteroatom Chem 21:343–350, 2010; Published online in Wiley InterScience ( www.interscience.wiley.com ). DOI 10.1002/hc.20607" @default.
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- W2131032741 date "2010-01-01" @default.
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- W2131032741 title "Tetraphenylphosphonium salts of N-thiophosphorylated thiobenzamide, mono-thioureas or bis-thioureas" @default.
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- W2131032741 doi "https://doi.org/10.1002/hc.20607" @default.
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