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- W2131777235 abstract "Reduction of (3S)-N,N-dibenzylamino-2-ketophosphonates 9a-d derived from L-amino acids was carried out with catecholborane at -20 o C to afford the (3S)-N,N-dibenzylamino-(2R)-hydroxy-phos- phonates syn-10a-d, whereas the reduction of (3S)-N-benzylamino-2- ketophosphonates 13a-d with Zn(BH4)2 at -78 o C yield (3S)-N-benzy- lamino-(2S)-hydroxyphosphonates anti-14a-d. The reduction in both cases was in good chemical yields and with high diastereoselectivity. The hydrolysis and hydrogenolysis of 10a-d and 14a-d afford the (3S)-amino-(2R)-hydroxyphosphonic acids 6 and (3S)-amino-(2S)- hydroxyphosphonic acids 7, respectively, which are analogues of phosphostatine." @default.
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- W2131777235 date "2005-01-01" @default.
- W2131777235 modified "2023-09-24" @default.
- W2131777235 title "Preparation of Phosphostatine Analogues From L-amino acids" @default.
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- W2131777235 doi "https://doi.org/10.29356/jmcs.v49i4.1321" @default.
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