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• W2131862783 abstract "Nanoporous silica was prepared and functionalized with amino propyl‐triethoxysilane to be used as a highly porous fiber‐coating material for solid‐phase microextraction ( SPME ). The prepared nanomaterials were immobilized onto a stainless steel wire for fabrication of the SPME fiber. The proposed fiber was evaluated for the extraction of volatile component of C itrus aurantium L . leaves. A homemade microwave‐assisted extraction followed by headspace ( HS ) solid‐phase apparatus was used for the extraction of volatile components. For optimization of factors affecting the extraction efficiency of the volatile compounds, a simplex optimization method was used. The repeatability for one fiber ( n = 4), expressed as RSD , was between 3.1 and 8.6% and the reproducibility for five prepared fibers was between 10.1 and 14.9% for the test compounds. Using microwave‐assisted distillation HS‐SPME followed by GC‐MS , 53 compounds were separated and identified in C . aurantium L., which mainly included limonene (62.0%), linalool (7.47%), trans ‐β‐Ocimene (3.47%), and caryophyllene (2.05%). In comparison to a hydrodistillation method, the proposed technique could equally monitor almost all the components of the sample, in an easier way, which was rapid and required a much lower amount of sample." @default.
• W2131862783 created "2016-06-24" @default.
• W2131862783 creator A5001592284 @default.
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• W2131862783 date "2013-03-01" @default.
• W2131862783 modified "2023-10-18" @default.
• W2131862783 title "Analysis of volatile oil composition of <i>Citrus aurantium</i> L. by microwave-assisted extraction coupled to headspace solid-phase microextraction with nanoporous based fibers" @default.
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• W2131862783 doi "https://doi.org/10.1002/jssc.201200674" @default.
• W2131862783 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/23483734" @default.
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