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- W2132898904 abstract "Dark brown crystals of [NPr4]2[TeBr6(SeBr2)2] (1) were obtainedwhen selenium and bromine (1:1) were allowed to react inacetonitrile solution in the presence of tellurium(IV) bromideand tetrapropylammonium bromide. The salt 1 crystallizes in themonoclinic space group P21/n with the cell dimensions a =14.7870(3)A, b = 9.5523(3)A, c = 16.7325(3)A, beta =110.56(10)deg (at 123(2) K). In the solid state the[TeBr6(SeBr2)2]2- anion contains a nearly regular [TeBr6]octahedron in which the four equatorial bromo ligands havedeveloped bonds to Se(II) atoms of the SeBr2 molecules. Thecontacts between the bridging bromo and the Se(II) atoms of theSeBr2 molecules are 3.0000(4) and 3.0561(4)A, and can beinterpreted as bonds of the donor-acceptor type with thebridging bromo ligands as donors and the SeBr2 molecules asacceptors. The Te(IV)-Br distances are in the range2.6816(3)-2.7131(3)A and the Se(II)-Br bond lengths in thecoordinated SeBr2 molecules are 2.3548(4) and 2.3725(4)A." @default.
- W2132898904 created "2016-06-24" @default.
- W2132898904 creator A5024192293 @default.
- W2132898904 creator A5053401652 @default.
- W2132898904 date "2008-11-25" @default.
- W2132898904 modified "2023-09-26" @default.
- W2132898904 title "ChemInform Abstract: Synthesis and Crystal Structure of Bis(tetrapropylammonium) Hexabromotellurate(IV)-bis{dibromoselenate(II)}, [NnPr4]2[TeBr6(SeBr2)2], the Salt of a Mixed-Valence Bromotellurate(IV)-Selenate(II) Anion." @default.
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- W2132898904 doi "https://doi.org/10.1002/chin.200848019" @default.
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