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- W2132988278 abstract "(3R,4S,5R)-3,4-O-Cyclohexylidene-3,4,5-trihydroxycyclohexan-1-one (11a), prepared from D-quinic acid (4a) by a published three-step sequence, was converted into the 5-O-benzoyl derivative (11b) by the action of benzoyl chloride. Simultaneous protection of the ketonic carbonyl group and removal of the cyclohexylidene moiety occurred when the compound (11b) was treated with ethane-1,2-dithiol and boron trifluoride–diethyl ether. The derived (7R,8R,9R)-9-benzoyloxy-7,8-dihydroxy-1,4-dithiaspiro-[4.5]decane (15a), when treated sequentially with lead(IV) acetate and pyrrolidinium acetate, underwent an oxidative ring contraction to give (8R)-8-benzoyloxy-1,4-dithiaspiro[4.4]non-6-ene-6-carbaldehyde (17a)." @default.
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- W2132988278 date "1983-01-01" @default.
- W2132988278 modified "2023-09-27" @default.
- W2132988278 title "Studies related to cyclopentanoid natural products. Part 2. An improved route to (4R)-4-hydroxy-2-hydroxymethylcyclopent-2-en-1-one and its O-substituted derivatives" @default.
- W2132988278 doi "https://doi.org/10.1039/p19830002441" @default.
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