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• W2133226112 abstract "RATIONALE Oxygen triple isotope compositions give key information for understanding physical processes during isotopic fractionation between the geo-, hydro-, bio-, and atmosphere. For detailed discussion of these topics, it is necessary to determine precise 17O-excess values of terrestrial silicate/oxide minerals with respect to Vienna Standard Mean Ocean Water (VSMOW). METHODS Water was fluorinated in an electrically heated Ni-metal tube into which water and BrF5 were loaded for the quantitative extraction of oxygen. Silicate/oxide minerals were fluorinated by heating with a CO2 laser in an atmosphere of BrF5. The extracted oxygen was purified and isotope ratios of the oxygen triple isotope compositions were determined using a Finnigan MAT253 isotope ratio mass spectrometer. RESULTS The oxygen triple isotope compositions of meteoric water and terrestrial silicate/oxide minerals fall on statistically distinguishable fractionation lines, defined as [ln(δ17O + 1) = λln(δ18O + 1) + Δ], where λ and Δ correspond to the slope and intercept, respectively. The fractionation line for meteoric water has λ = 0.5285 ± 0.0005 and Δ = 0.03 ± 0.02‰ and for terrestrial silicate/oxide minerals has λ = 0.5270 ± 0.0005 and Δ = –0.070 ± 0.005‰, at the 95% confidence limit. CONCLUSIONS All the analyzed terrestrial silicate/oxide minerals including internationally accepted reference materials (NBS-28, UWG-2, and San Carlos olivine) have a negative 17O-excess with respect to VSMOW. We propose that it is necessary to specify if the determined δ17O values of terrestrial and extraterrestrial samples are expressed as the difference from VSMOW or the terrestrial silicate mineral-corrected value. Copyright © 2012 John Wiley & Sons, Ltd." @default.
• W2133226112 created "2016-06-24" @default.
• W2133226112 creator A5044114731 @default.
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• W2133226112 date "2012-12-13" @default.
• W2133226112 modified "2023-10-04" @default.
• W2133226112 title "Determination of ¹⁷ O-excess of terrestrial silicate/oxide minerals with respect to Vienna Standard Mean Ocean Water (VSMOW)" @default.
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• W2133226112 doi "https://doi.org/10.1002/rcm.6453" @default.
• W2133226112 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/23239376" @default.
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