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- W2133477828 abstract "ABSTRACT A rapid, simple and reliable method was devised for separation and determination of six metal cations, based on the capillary zone electrophoresis. The results showed that the complete separation of K + ,Cu 2+ , Zn 2+ , Mn , Pb 2+ and Cd 2+ can be achieved within 5 min. A new electrolyte system containing 15 mmol·L -1 imidazole as a background absorbance reference and 8 mmol·L -1 malonic acid, 2 mmol·L -1 18-crown-6 ether as the complexing agents, 10% methanol as an organic modifier, by using acetic acid to adjust the pH=4.40 was developed. The applied voltage was 20 kV at 25 o C. Under the optimum conditions, 6 ions were separated and determined with the correlation coefficient of 0.9984-0.9993. The detection limits (S/N=3) from 0.05 (K + ) to 0.75 (Zn 2+ ) mg·L -1 . The repeatability of migration times was less than 0.60% and of peak area ranged from 3.4 to 5.6% (n=6). The results were compared with AAS for analyzing the real samples of waste-water and snow water. Keywords: Electrolyte composition; metal cations; capillary zone electrophoresis" @default.
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- W2133477828 date "2008-03-01" @default.
- W2133477828 modified "2023-10-12" @default.
- W2133477828 title "SEPARATION AND DETERMINATION OF SIX METAL CATIONS BY CAPILLARY ZONE ELECTROPHORESIS" @default.
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- W2133477828 doi "https://doi.org/10.4067/s0717-97072008000100020" @default.
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