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- W2133609551 abstract "Mechanical high energy ball milling of an Fe+2Si elemental powders mixture was used to activate a self sustaining combustion reaction or so-called self-propagating high-temperature synthesis (SHS) to form iron disilicide, a reaction for which the thermodynamic criterion is not favorable. A complete characterization of the milled powders before reaction was performed with energy dispersive X-ray spectrometry, specific surface measurements and X-ray diffraction profile analysis. Thermal and structural information describing the combustion front initiated by heating up a sample to 400°C in a Fe–Si system is communicated. In order to isolate the phases involved in the gasless reaction, a time-resolved X-ray diffraction experiment was designed to study in situ the formation of silicide phases (FeSi and β-FeSi2) produced by the new process called MASHS (mechanically activated self-propagating high-temperature synthesis)." @default.
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- W2133609551 date "1999-05-01" @default.
- W2133609551 modified "2023-10-16" @default.
- W2133609551 title "Enhancement of self-sustaining reaction by mechanical activation: case of an FeSi system" @default.
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- W2133609551 doi "https://doi.org/10.1016/s0921-5093(98)01108-3" @default.
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