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- W2133834118 abstract "Thermolysis of benz[cd]indazole 1,2-dioxide at 105–110 °C in the presence of various benzenoid derivatives gave benz[cd]indazole 1-oxide and oxidation products of the benzenoid substrates. Toluene was oxidised to benzyl alcohol (40% yield based on the dioxide), benzaldehyde (19%), benzoic acid (0.5%), o-cresol (11%), m-cresol (3%), and p-cresol ([graphic omitted]4%); an experiment with [4-3H]toluene showed no appreciable migration and retention of tritium (NIH shift) during formation of p-cresol. [4-2H]Anisole was converted mainly into deuteriated phenol (14%) and 2-hydroxyanisole (13%) together with 4-hydroxyanisole (4%) containing no significant amounts of deuterium. Naphthalene gave α- and β-naphthol in low yield. In contrast, 4-methylcinnoline 1,2-dioxide was stable in hot anisole. The results are compared with those reported for other, related oxidising systems." @default.
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- W2133834118 date "1976-01-01" @default.
- W2133834118 modified "2023-09-26" @default.
- W2133834118 title "Thermal oxygen atom transfer from benz[cd]indazole 1,2-dioxide to benzenoid derivatives" @default.
- W2133834118 doi "https://doi.org/10.1039/p19760000680" @default.
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