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- W2133996919 abstract "The combustion synthesis of the common ferroelectric material, BaTiO 3 , was developed using the stoichiometry: BaO 2 +0.2 Ti +0.8 TiO 2 → BaTiO 3 +0.3 O 2 . An adiabatic temperature, T ad , of the reaction was calculated from known thermodynamic data to be 1917 °C. Real time chemical changes in the formation of BaTiO 3 during the reaction have been monitored using time-resolved X-ray diffraction with synchrotron radiation as the X-ray source. A time resolution of 250 ms was achieved. The combustion synthesis of BaTiO 3 was followed by observing the intensities of reactant and product Bragg diffraction peaks in order to qualitatively identify the phases present. Because BaTiO 3 forms initially as a cubic phase, X-ray diffraction of the product was monitored for a period of 20 min after the reaction to observe the phase transformation to the tetragonal form. This transformation is evident in these post-reaction scans as the cubic 110 and 220 peaks are split to the tetragonal 101/110 and 202/220 ones, respectively." @default.
- W2133996919 created "2016-06-24" @default.
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- W2133996919 date "1999-06-01" @default.
- W2133996919 modified "2023-09-24" @default.
- W2133996919 title "The combustion synthesis of the ferroelectric material, BaTiO3, studied by time-resolved X-ray diffraction" @default.
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- W2133996919 doi "https://doi.org/10.1017/s0885715600010381" @default.
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