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- W2134137246 endingPage "2022" @default.
- W2134137246 startingPage "2015" @default.
- W2134137246 abstract "In the presence of titanium(IV) tetraethoxide ((EtO)4Ti), menthyl arylglyoxylates are prepared by transesterification of ethyl arylglyoxylates and natural (−)-(1R,2S,5R)-menthol. Using menthyl as a chiral auxiliary, the corresponding novel (R)-menthyl 2-aryl-2-hydroxybutanoates are synthesized by the addition of Et2Zn with menthyl arylglyoxylates. The structures of the products are characterized by IR and 1H- and 13C-NMR spectroscopy, mass spectrometry, and elemental analysis. The diastereoselectivities are analyzed by HPLC. The addition reactions are completed with good yields and high diastereoisomeric excess (de up to 95%), and, after hydrolysis, the (R)-2-aryl-2-hydroxybutanoic acids are obtained with high optical purities." @default.
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- W2134137246 date "2010-10-01" @default.
- W2134137246 modified "2023-09-26" @default.
- W2134137246 title "The Stereoselective Synthesis of 2-Aryl-2-hydroxybutanoic Acid via Menthyl Chiral Auxiliaries" @default.
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- W2134137246 doi "https://doi.org/10.1002/hlca.201000024" @default.
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